HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 23047606, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 16769476 | HCID 16769476 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 23047606 | HCID 23047606 | — |
Reaction Steps
Following a procedure similar to that described in Preparation 44, the desired compound was prepared from 6.12 g of 2-(o-toluidino)thiazole-4-ylmethanol, 13.2 g of a sulfur trioxide pyridine complex, 12 ml of triethylamine and 210 ml of dimethyl sulfoxide, as pale brown prismatic crystals having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-f4d5b64d9b4944fab3df556a8f2e963a |
| Source note | uspto-grants-1990_06 |