HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(cyclohexylamino)-1,3-thiazole-4-carboxylate → 2-Cyclohexylaminothiazol-4-ylmethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(cyclohexylamino)-1,3-thiazole-4-carboxylate | HCID 15053542 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 2-Cyclohexylaminothiazol-4-ylmethanol | HCID 15053560 | — |
Reaction Steps
The reaction described in Preparation 15 was repeated, but using 19 g of ethyl 2-cyclohexylaminothiazole-4-carboxylate, 4.2 g of lithium aluminum hydride and 250 ml of tetrahydrofuran, giving the title compound as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-89bae77397e94dfe9821863506d66151 |
| Source note | uspto-grants-1990_06 |