HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → Ethyl 2-(morpholin-4-yl)-1,3-thiazole-4-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Ethyl 2-chlorothiazole-4-carboxylate | HCID 13106141 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | Ethyl 2-(morpholin-4-yl)-1,3-thiazole-4-carboxylate | HCID 15053544 | — |
Reaction Steps
The reaction described in Preparation 26 was repeated, but using 1.4 g of morpholine, 3 g of ethyl 2-chlorothiazole-4-carboxylate. 3 g of triethylamine and 12 ml of dimethylformamide, giving the title compound as colorless needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-b46b1738171d4f99b3f6b71f8b2ba682 |
| Source note | uspto-grants-1990_06 |