HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → 2-(Morpholin-4-yl)-1,3-thiazole-4-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | [2-(Morpholin-4-yl)-1,3-thiazol-4-yl]methanol | HCID 10608093 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 2-(Morpholin-4-yl)-1,3-thiazole-4-carbaldehyde | HCID 15053579 | — |
Reaction Steps
The reaction described in Preparation 44 was repeated but using 2.4 g of 2-morpholinothiazol-4-ylmethanol, 5.7 g of sulfur trioxide pyridine complex. 3.6 g of triethylamine and 30 ml of dimethyl sulfoxide, giving the title compound as pale yellow needles.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-d26199f514254cbfbaf176d910527013 |
| Source note | uspto-grants-1990_06 |