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HRID2107290

反应详情

EQUATION

反应方程式

HRID 2107290 的结构方程式

REACTANTS

反应物

2
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：OCc1csc(N2CCOCC2)n1
HCID10608093

[2-(Morpholin-4-yl)-1,3-thiazol-4-yl]methanol

C8H12N2O2S

PRODUCTS

生成物

1
结构：O=Cc1csc(N2CCOCC2)n1
HCID15053579

2-(Morpholin-4-yl)-1,3-thiazole-4-carbaldehyde

C8H10N2O2S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

The reaction described in Preparation 44 was repeated but using 2.4 g of 2-morpholinothiazol-4-ylmethanol, 5.7 g of sulfur trioxide pyridine complex. 3.6 g of triethylamine and 30 ml of dimethyl sulfoxide, giving the title compound as pale yellow needles.

WORKUP

后处理

  1. customThe reaction described in Preparation 44