Triethylamine → HCID 15053581, compound

HRID 2107296Notes

Reaction equation

HRID 2107296 reaction equation
[N:1]1([C:7]2[S:8][CH:9]=[C:10]([CH2:12][OH:13])[N:11]=2)[CH2:6][CH2:5][S:4][CH2:3][CH2:2]1.C(N(CC)CC)C>CS(C)=O>[N:1]1([C:7]2[S:8][CH:9]=[C:10]([CH:12]=[O:13])[N:11]=2)[CH2:6][CH2:5][S:4][CH2:3][CH2:2]1

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 15053563HCID 15053563, compound

Product 1

HCID 15053581HCID 15053581, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

The reaction described in Preparation 44 was repeated, but using 1.2 g of 2-(thiomorpholin-4-yl)thiazol-4-ylmethanol, 2.65 g of sulfur trioxide pyridine complex, 1.68 g of triethylamine and 30 ml of dimethyl sulfoxide, giving the title compound as a colorless powder.

Workup

  1. customThe reaction described in Preparation 44

Sources & evidence

ORD record
ord-eed5622d70a34a3bb1da49ceb16e0565
Source dataset
uspto-grants-1990_06
Patent number
US04933355

Reaction notes

Loading…