HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15053547, compound → HCID 15053564, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15053547 | HCID 15053547 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 15053564 | HCID 15053564 | — |
Reaction Steps
The reaction described in Preparation 15 was repeated, but using 4.0 g of ethyl 2-(4-methyl-1-piperazinyl)-thiazole-4-carboxylate, 0.6 g of lithium aluminum hydride and 50 ml of tetrahydrofuran, giving the title compound as white prisms.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-feb5f56f3a72443b9987008521f7e3d8 |
| Source note | uspto-grants-1990_06 |