Aluminium lithium hydride → HCID 15053565, compound

HRID 2107300Notes

Reaction equation

HRID 2107300 reaction equation
[CH2:1]([NH:9][C:10]1[S:11][CH:12]=[C:13]([C:15]([O-])=[O:16])[N:14]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].[H-].[Al+3].[Li+].[H-].[H-].[H-]>O1CCCC1>[CH2:1]([NH:9][C:10]1[S:11][CH:12]=[C:13]([CH2:15][OH:16])[N:14]=1)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

4

Reactant 2

HCID 21226445Aluminium lithium hydrideHCID 23047652HCID 23047652, compound

Product 1

HCID 15053565HCID 15053565, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The reaction described in preparabion 15 was repeated, but using 1.5 g of 2-octylaminothiazol-4-carboxylate, 0.2 g of lithium aluminum hydride and 30 ml of tetrahydrofuran, giving the title compound as a pale yellow oil.

Sources & evidence

ORD record
ord-031c8d7687714ba6bb66d788c3a92225
Source dataset
uspto-grants-1990_06
Patent number
US04933355

Reaction notes

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