HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropylamine → HCID 15053551, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropylamine | HCID 69828 | — |
| Reactant | Ethyl 2-bromo-1,3-thiazole-4-carboxylate | HCID 353965 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15053551 | HCID 15053551 | — |
Reaction Steps
The reaction described in Preparation 26 was repeated, except that a mixture comprising 2.28 g of cyclopropylamine, 5.0 g of ethyl 2-bromothiazole-4-carboxylate and 20 ml of toluene was heated at 100°-110 ° C. for 16 hours in a sealed tube, giving the title compound as a pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04933355 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-8c672ab097c242b4980545ce709da6e2 |
| Source note | uspto-grants-1990_06 |