HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-butyryl-3-ethoxyacrylate → ethyl 2-[[(4-methoxythiophen-3-yl)amino]methylidene]-3-oxohexanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-butyryl-3-ethoxyacrylate | HCID 3359484 | — |
| Reactant | 4-Methoxythiophen-3-amine | HCID 14989685 | — |
| Product | ethyl 2-[[(4-methoxythiophen-3-yl)amino]methylidene]-3-oxohexanoate | HCID 178450504 | — |
Reaction Steps
4-Methoxy-3-thiopheneamine (11 g, 0.085 mol) and ethyl 2-butyryl-3-ethoxyprop-2-enoate (20 g, 0.093 mol) was heated in an inert atmosphere at 120° for 30 minutes. Addition of petroleum ether, b.p. 40°-60°, 200 ml, gave a solid which was collected by filtration and dried, 17.58 g, m.p. 89°-91°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04935431 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-13e10781fd984666a98a8ff8db638f61 |
| Source note | uspto-grants-1990_06 |