HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15117875, compound → HCID 15117876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15117875 | HCID 15117875 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 15117876 | HCID 15117876 | 116% |
Reaction Steps
A mixture of 4 g (9.1 mmole) of 1-benzyloxy-2-(5-hydroxymethyl-2-methyl-2-tetrahydrofuranylmethoxy)-4-t-octylbenzene, 1 g of 10% palladium-on-carbon and 75 ml of ethanol was shaken under an atmosphere of hydrogen at ca. 4 kg/cm2 for 3 hours. The resulting mixture was filtered, and the filtrate was evaporated in vacuo to give 3.7 g of the title compound as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04935442 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-63ff32eefa76456cbeacdbd9398ba988 |
| Source note | uspto-grants-1990_06 |