Hydrochloric Acid → HCID 15117892, compound

Participants

Reaction Steps

The above benzaldehyde was dissolved in methanol (400 ml) containing 1N hydrochloric acid (50 ml) and the mixture was stirred at room temperature for 3 hours. The methanol was removed by evaporation in vacuo, and the residue was extracted with dichloromethane. The extracts were evaporated in vacuo, to give the title compound as an oil (23.6 g).

Provenance & Evidence