Hydrochloric Acid → HCID 15117892, compound

HRID 2107751Notes

Reaction equation

HRID 2107751 reaction equation
O1CCCCC1[O:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[CH:21]=[CH:20][C:19]([C:22]([CH2:25][C:26]([CH3:29])([CH3:28])[CH3:27])([CH3:24])[CH3:23])=[CH:18][C:15]=1[CH:16]=[O:17].Cl>CO>[OH:7][CH2:8][CH2:9][O:10][CH2:11][CH2:12][O:13][C:14]1[CH:21]=[CH:20][C:19]([C:22]([CH2:25][C:26]([CH3:29])([CH3:28])[CH3:27])([CH3:23])[CH3:24])=[CH:18][C:15]=1[CH:16]=[O:17]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 15117891HCID 15117891, compound

Product 1

HCID 15117892HCID 15117892, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

The above benzaldehyde was dissolved in methanol (400 ml) containing 1N hydrochloric acid (50 ml) and the mixture was stirred at room temperature for 3 hours. The methanol was removed by evaporation in vacuo, and the residue was extracted with dichloromethane. The extracts were evaporated in vacuo, to give the title compound as an oil (23.6 g).

Workup

  1. customThe methanol was removed by evaporation in vacuo
  2. extractionthe residue was extracted with dichloromethane
  3. customThe extracts were evaporated in vacuo

Sources & evidence

ORD record
ord-99be7ac57efe4fd2a0924b0ebc72a347
Source dataset
uspto-grants-1990_06
Patent number
US04935442

Reaction notes

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