HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 23673134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14075347 | HCID 14075347 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 23673134 | HCID 23673134 | 88% |
Reaction Steps
0.42 g (0.0052 mol) of 50% aqueous sodium hydroxide is added to a suspension of 1.6 g (0.0052 mol) 6-(4-chlorophenyl)-1-methyl-2-n-propyl-4-oxonicotinic acid in 25 ml of methanol. The solution formed is allowed to stand at room temperature for 1 hr. and is concentrated in vacuo. The concentrate is dried to afford 1.5 g (88% yield) of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04936904 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-ea9e5882477940f3928c4fcb6dfe63ee |
| Source note | uspto-grants-1990_06 |