HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 14075369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 14075269 | HCID 14075269 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 14075369 | HCID 14075369 | — |
Reaction Steps
3.0 gms of 2,6-diphenyl-3-methoxycarbonyl-pyr-4-one, 33 mls of methanol, 13.3 mls of 40% aqueous methylamine and 2 mls of glacial acetic acid were mixed at room temperature. The next day the mixture was diluted with water. Filtration of the resulting suspension yielded 2.5 gms of methyl 2,6-diphenyl-1-methyl-4-oxonicotinate. Recrystallization from methanol provided material at 255°-7°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04936904 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-86b36515f1c64df9a14d08793d66a84a |
| Source note | uspto-grants-1990_06 |