HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloropyridine → HCID 23045000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloropyridine | HCID 27685 | — |
| Reactant | 1-(4,4-Bis(4-fluorophenyl)butyl)piperazine | HCID 79729 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 23045000 | HCID 23045000 | — |
Reaction Steps
19.8 g (0.06 mole) of 1-[4,4-bis(p-fluorophenyl)butyl]-piperazine and 2.96 g (0.02 mole) of 2,5-dichloropyridine were heated together with 2 ml of toluene at 130° C. (temperature of oil bath) for 20 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04937245 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-527650e0dea040baaca100bd8b6b8ef4 |
| Source note | uspto-grants-1990_06 |