HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargyl bromide → HCID 23045087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargyl bromide | HCID 7842 | — |
| Reactant | Pyripropanol | HCID 72922 | — |
| Product | HCID 23045087 | HCID 23045087 | — |
Reaction Steps
From 2-pyridinepropanol (13.7 g) and propargyl bromide (80% solution in toluene, 12 ml), with a reaction time of 2 h. FCC eluting with hexane-ether (1:1) gave the title compound as an orange oil (9.0 g), t.l.c. (System B 80:20:1) Rf 0.15.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04937251 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-833aca8dc2da4ed79d1b419315306ce4 |
| Source note | uspto-grants-1990_06 |