1,6-Dibromohexane → HCID 23045066, compound

HRID 2108024Notes

Reaction equation

HRID 2108024 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH2:7][CH2:8][CH2:9][CH2:10][OH:11].[Br:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18]Br>>[Br:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][O:11][CH2:10][CH2:9][CH2:8][CH2:7][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1

Participants

3

Reactant 2

HCID 123681,6-DibromohexaneHCID 232734664-(Pyridin-2-yl)butan-1-ol

Product 1

HCID 23045066HCID 23045066, compound

Procedure

From 2-pyridinebutanol (3.96 g) and 1,6-dibromohexane (15 ml), with a reaction time of 4 h. FCC eluting with hexane→ether gave the title compound as a pale yellow oil (3.7 g), t.l.c. (hexane-diethyl ether 1:1) Rf 0.22.

Workup

  1. customwith a reaction time of 4 h
  2. washFCC eluting with hexane→ether

Sources & evidence

ORD record
ord-9eaa72e0d045441ba12a4cffbc968a0b
Source dataset
uspto-grants-1990_06
Patent number
US04937251

Reaction notes

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