HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,6-Dibromohexane → HCID 23045066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,6-Dibromohexane | HCID 12368 | — |
| Reactant | 4-(Pyridin-2-yl)butan-1-ol | HCID 23273466 | — |
| Product | HCID 23045066 | HCID 23045066 | — |
Reaction Steps
From 2-pyridinebutanol (3.96 g) and 1,6-dibromohexane (15 ml), with a reaction time of 4 h. FCC eluting with hexane→ether gave the title compound as a pale yellow oil (3.7 g), t.l.c. (hexane-diethyl ether 1:1) Rf 0.22.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04937251 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-9eaa72e0d045441ba12a4cffbc968a0b |
| Source note | uspto-grants-1990_06 |