HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Hydroxyethyl)pyridine → HCID 23045065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Hydroxyethyl)pyridine | HCID 7675 | — |
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Product | HCID 23045065 | HCID 23045065 | — |
Reaction Steps
From 2-pyridineethanol (5.0 g) and 1,5-dibromopentane (16.6 ml), with a reaction time of 4 h. FCC eluting with hexane-diethyl ether (1:0→1:1) gave the title compound as a colourless oil (6.15 g), t.l.c. (ether-hexane 1:1) Rf 0.19.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04937251 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-1419ca70c8ed4e73b79da6473ad6466e |
| Source note | uspto-grants-1990_06 |