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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2108026Generated: October 26, 2026

1,6-Dibromohexane → HCID 23045054, compound

https://huagongshe.com/reaction/2108026

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,6-DibromohexaneHCID 12368—
Reactant5-Bromo-2-pyridinepropanolHCID 13979735—
ProductHCID 23045054HCID 2304505468.4%

Reaction Steps

From 3-(5-bromo-2-pyridinyl)propanol (2 g) and 1,6-dibromohexane (6.77 g) with a reaction time of 3 h. FCC eluting with hexane→hexane:ether (100:0→90:10) gave the title compound as a yellow oil (2.4 g), t.l.c. (hexane:ether 9:1) Rf 0.08.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04937251
Source datasetuspto-grants-1990_06
ORD IDord-b533c398a9034640a35fab2f788bc499
Source noteuspto-grants-1990_06