HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70361905, compound → HCID 23045076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70361905 | HCID 70361905 | — |
| Catalyst | Palladium monoxide | HCID 5083724 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23045076 | HCID 23045076 | 99.7% |
Reaction Steps
(Z)-2-[4-[(6-Bromohexyl)oxy]-1-butenyl]-3-(phenylmethoxy)pyridine (1.5 g) was hydrogenated over pre-reduced 10% palladium oxide on carbon (50% aqueous paste, 300 mg) in ethanol (15 ml). The catalyst was removed by filtration through hyflo and the solvent was evaporated to give the title compound as a yellow oil (1.18 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04937251 |
| Source dataset | uspto-grants-1990_06 |
| ORD ID | ord-111056d87a1740b4b9fe03eafc592bb3 |
| Source note | uspto-grants-1990_06 |