反应详情

A solution of 3-[[2-[(6-bromohexyl)oxy]ethyl]oxy]pyridine (2 g) and benzylamine (10 ml) was stirred at 140° under nitrogen for 3 h. The solution was partitioned between 8% sodium bicarbonate (100 ml) and ethylacetate (100 ml). The organic extract was dried and distilled to give the title compound (1.8 g) as an oil. T.l.c. (System B 80:20:1) Rf 0.54

1. customThe solution was partitioned between 8% sodium bicarbonate (100 ml) and ethylacetate (100 ml)
2. extractionThe organic extract
3. customwas dried
4. distillationdistilled