Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzylamine → HCID 23045290, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | 3-[2-[(6-Bromohexyl)oxy]ethoxy]pyridine | HCID 23045265 | — |
| 생성물 | HCID 23045290 | HCID 23045290 | — |
반응 단계
A solution of 3-[[2-[(6-bromohexyl)oxy]ethyl]oxy]pyridine (2 g) and benzylamine (10 ml) was stirred at 140° under nitrogen for 3 h. The solution was partitioned between 8% sodium bicarbonate (100 ml) and ethylacetate (100 ml). The organic extract was dried and distilled to give the title compound (1.8 g) as an oil. T.l.c. (System B 80:20:1) Rf 0.54
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04937268 |
| 출처 데이터셋 | uspto-grants-1990_06 |
| ORD ID | ord-861d08ece5bb41368b39f417691c1854 |
| 출처 메모 | uspto-grants-1990_06 |