HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,4,4-Trifluoro-1-(m-tolyl)butane-1,3-dione → HCID 67213403, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,4,4-Trifluoro-1-(m-tolyl)butane-1,3-dione | HCID 18624099 | — |
| Reactant | HCID 178510443 | HCID 178510443 | — |
| Product | HCID 67213403 | HCID 67213403 | 54.3% |
Reaction Steps
Reaction of 1-(3-methyl-phenyl)-4,4,4-trifluoro-butane-1,3-dione (230 mg, 1.0 mmol), prepared from commercially available 3-methyl-acetophenone according to general procedure A, and 3-amino-4-cyano-pyrazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as a yellow solid (164 mg, 54%). MS (ISP) 303.2 [(M+H)+]; mp 202° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514443B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-fb020c6ca5dc4368a757940448321bef |
| Source note | uspto-grants-2009_04 |