HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluoro-1-phenylethan-1-one → HCID 67212987, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluoro-1-phenylethan-1-one | HCID 9947 | — |
| Reactant | 4,4,4-trifluoro-1-(2-fluorophenyl)butane-1,3-dione | HCID 43186919 | — |
| Reactant | HCID 178510443 | HCID 178510443 | — |
| Product | HCID 67212987 | HCID 67212987 | 27.1% |
Reaction Steps
Reaction of 1-(2-fluoro-phenyl)-4,4,4-trifluoro-butane-1,3-dione (234 mg, 1.0 mmol), prepared from commercially available 2-fluoro-acetophenone according to general procedure A, and 3-amino-4-cyano-pyrazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as a light yellow solid (83 mg, 27%). MS (ISP) 307.1 [(M+H)+]; mp 165° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514443B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-da7c7c6ec23343dfa0de031e32b0cf8a |
| Source note | uspto-grants-2009_04 |