HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetophenone → HCID 11196973, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetophenone | HCID 7410 | — |
| Reactant | 4,4,4-Trifluoro-1-phenyl-1,3-butanedione | HCID 67589 | — |
| Reactant | 5-amino-1H-imidazole-4-carbonitrile | HCID 78777 | — |
| Product | HCID 11196973 | HCID 11196973 | 37.1% |
Reaction Steps
Reaction of 1-phenyl-4,4,4-trifluoro-butane-1,3-dione (216 mg, 1.0 mmol), prepared from commercially available acetophenone according to general procedure A, and 4-amino-5-cyano-1H-imidazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as a yellow solid (107 mg, 37%). MS (ISP) 289.0 [(M+H)+]; mp 202° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514443B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-0a8272c4eb6645159e31a236deaf35d3 |
| Source note | uspto-grants-2009_04 |