HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenyl-1-propanone → HCID 67213025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenyl-1-propanone | HCID 7148 | — |
| Reactant | 5-amino-1H-imidazole-4-carbonitrile | HCID 78777 | — |
| Reactant | 4,4,4-Trifluoro-1-(2-methylphenyl)butane-1,3-dione | HCID 15772021 | — |
| Product | HCID 67213025 | HCID 67213025 | 6.3% |
Reaction Steps
Reaction of 1-(2-methyl-phenyl)-4,4,4-trifluoro-butane-1,3-dione (230 mg, 1.0 mmol), prepared from commercially available 2-methyl-acetophenone according to general procedure A, and 4-amino-5-cyano-1H-imidazole (108 mg, 1.0 mmol) according to general procedure B yielded the title compound as a yellow solid (19 mg, 6%). MS (ISP) 303.0 [(M+H)+]; mp 151° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514443B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-1f44ad8efd3a4194a093496492a43965 |
| Source note | uspto-grants-2009_04 |