Ethyl Acetate → HCID 66643053, compound

Participants

Reaction Steps

3,5-dimethyl-4-(4′-hydroxy-3′-iso-propyl-phenylsulfanyl)phenol was prepared from 2,5-dimethyl-4-(3′-iso-propyl-4′-methoxy-phenylsulfanyl)-anisole according to the procedure described in example 8, step d. 1H NMR (300 MHz, DMSO-d6): δ 9.58(bs, 1H), 9.21(bs, 1H), 6.77(m, 1H), 6.63(m, 3H), 6.46(dd, 1H, J=2.7 Hz and J=8.1 Hz), 3.09(m, 1H), 2.28(s, 6H), 1.06(d, 6H, J=7.2 Hz); TLC conditions: Uniplate silica gel, 250 microns; Mobile phase=ethyl acetate 25% in hexane; Rf=0.12

Provenance & Evidence