反应详情

tert-Butyl 4-(1-tosyl-1H-pyrrolo[2,3-b]pyridin-3-yl)thiophen-2-ylcarbamate (120 mg, 0.26 mmol) was dissolved in 2 mL CH2Cl2, 2 mL TFA. After 15 minutes the reaction mixture was concentrated to an oil, dissolved in EtOAc, and washed with 0.1 NaOH. The organic layer was dried to a brown oil which was used as obtained.

1. concentrationAfter 15 minutes the reaction mixture was concentrated to an oil
2. dissolutiondissolved in EtOAc
3. washwashed with 0.1 NaOH
4. customThe organic layer was dried to a brown oil which
5. customas obtained