HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Chloro-2-(diethylamine)ethane hydrochloride → HCID 69065330, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Chloro-2-(diethylamine)ethane hydrochloride | HCID 13363 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 4-(Acetylamino)benzenesulfinic acid | HCID 412150 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 69065330 | HCID 69065330 | — |
Reaction Steps
9.0 g of 4-acetamido-phenylsulphinic acid are dissolved in 10 ml of water and 45 ml of 1N sodium hydroxide solution and 9.47 g of 2-chlorotriethylamine hydrochloride are added. The mixture is stirred for 5 hours at reflux temperature. After cooling, sodium hydroxide solution is added until an alkaline reaction is obtained, the mixture is extracted with ethyl acetate, dried over magnesium sulphate and finally the solvent is eliminated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514468B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-d6396b351f864c0abea1e4bff9a0de9c |
| Source note | uspto-grants-2009_04 |