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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2109378Generated: October 31, 2026

HCID 23062455, compound → HCID 23062408, compound

https://huagongshe.com/reaction/2109378

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 23062455HCID 23062455—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 23062408HCID 2306240899.1%

Reaction Steps

An ethanol (10 ml) solution of methyl 4-phenyl-3-vinyl-2-furancarboxylate (0.20 g) was blended with 10% palladium carbon and hydrogenated for 3 hours at 25° C. while stirring. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure, thereby giving 0.20 g of methyl 3-ethyl-4-phenyl-2-furancarboxylate. This compound was reacted with hydrazine monohydrate in the same manner as in Reference Example 31, thereby giving 0.12 g of the desired compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07514452B2
Source datasetuspto-grants-2009_04
ORD IDord-cb01beee402c420796cbcbb9d8756219
Source noteuspto-grants-2009_04