HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23062455, compound → HCID 23062408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23062455 | HCID 23062455 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 23062408 | HCID 23062408 | 99.1% |
Reaction Steps
An ethanol (10 ml) solution of methyl 4-phenyl-3-vinyl-2-furancarboxylate (0.20 g) was blended with 10% palladium carbon and hydrogenated for 3 hours at 25° C. while stirring. The catalyst was filtered off, and the filtrate was concentrated under reduced pressure, thereby giving 0.20 g of methyl 3-ethyl-4-phenyl-2-furancarboxylate. This compound was reacted with hydrazine monohydrate in the same manner as in Reference Example 31, thereby giving 0.12 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514452B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-cb01beee402c420796cbcbb9d8756219 |
| Source note | uspto-grants-2009_04 |