HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Bromo-4-methoxybenzoic acid → Ethyl 3-bromo-4-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Bromo-4-methoxybenzoic acid | HCID 66836 | — |
| Reactant | 3-Bromofuran-2-carboxylic acid | HCID 605479 | — |
| Product | Ethyl 3-bromo-4-methoxybenzoate | HCID 23062539 | — |
Reaction Steps
A reaction was carried out in the same manner as in Reference Example 1 except that the 3-bromo-2-furancarboxylic acid used in Reference Example 1 was replaced with 3-bromo-4-methoxybenzoic acid (4.62 g). The crude product was purified by silica gel column chromatography (eluent: ethyl acetate/hexane=1/10), thereby giving 4.65 g of ethyl 3-bromo-4-methoxybenzoate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514452B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-4b46e69b70fd4b4aa893cbd58bfefb1d |
| Source note | uspto-grants-2009_04 |