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HRID2109462

反应详情

EQUATION

反应方程式

HRID 2109462 的结构方程式

REACTANTS

反应物

2
结构：O=C1NC[C@@]2(CN3CCC2CC3)O1
HCID5310971

AR-R17779

C9H14N2O2

结构：Brc1coc(-c2ccncc2)c1
HCID57634253

4-(4-Bromofuran-2-yl)pyridine

C9H6BrNO

PRODUCTS

生成物

1
结构：O=C1O[C@]2(CN3CCC2CC3)CN1c1coc(-c2ccncc2)c1
HCID11232593

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[Cu][I]
催化剂HCID24350

Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI)

CuI

PROCEDURE

实验过程

The title compound was prepared by a method analogous to that described in Preparation 3 from (S)-spiro[1-azabicyclo[2.2.2]octan-3,5′-oxazolidin]-2′-one and 4-bromo-2-(4-pyridyl)furan using 4 equivalents of copper (I) iodide. The title compound (124 mg) was obtained as a pale yellow solid, m/z 342 (MH+).

WORKUP

后处理

  1. customThe title compound was prepared by a method analogous to