HRID2109473

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID5310971

AR-R17779

C9H14N2O2

HCID57634262

4-(5-Bromo-1,3,4-thiadiazol-2-yl)pyridine

C7H4BrN3S

PRODUCTS

生成物

结构：O=C1O[C@]2(CN3CCC2CC3)CN1c1nnc(-c2ccncc2)s1

HCID57634239

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID24350

Copper(1+) iodide; Copper(I) iodide; Cuprous iodide; Cuprous iodide (CuI)

CuI

PROCEDURE

实验过程

The compound was prepared by a method analogous to that described in Preparation 3 from (S)-spiro[1-azabicyclo[2.2.2]octan-3,5′-oxazolidin]-2′-one and 2-bromo-5-(4-pyridyl)-1,3,4-thiadiazole using 5 equivalents of copper (I) iodide. The title compound was obtained as a beige solid, m/z 344 (MH+).

WORKUP

后处理

customThe compound was prepared by a method analogous to