HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitrobenzenesulfonyl chloride → HCID 9871166, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| Reactant | 2'-(Aminomethyl)-N-(2-phenylethyl)[1,1'-biphenyl]-2-carboxamide | HCID 15509384 | — |
| Reactant | HCID 68973753 | HCID 68973753 | — |
| Product | HCID 9871166 | HCID 9871166 | — |
Reaction Steps
From 0.61 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid phenethylamide (precursor 5a) and 3-nitrophenylsulfonyl chloride, according to the general working procedure 272 mg of 2′-(3-nitrophenylsulfonyl-aminomethyl)biphenyl-2-carboxylic acid phenethylamide were obtained; m.p. 145° C. MS (ES+): m/e=516 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514582B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-5ababc9a6d6d4c33848d648405aa1796 |
| Source note | uspto-grants-2009_04 |