HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzenesulfonyl chloride → HCID 9804010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzenesulfonyl chloride | HCID 9588 | — |
| Reactant | 2'-Aminomethylbiphenyl-2-carboxylic acid (3-methylbutyl)amide | HCID 67316109 | — |
| Reactant | HCID 86589513 | HCID 86589513 | — |
| Product | HCID 9804010 | HCID 9804010 | — |
Reaction Steps
From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid (3-methyl-butyl)amide (precursor 5c) and 4-fluorophenylsulfonyl chloride, according to the general working procedure 122 mg of 2′-(4-fluorophenylsulfonyl-aminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained; m.p. 149° C. MS (ES+): m/e=455 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514582B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-d8974843d133474b908a9614e1e33b11 |
| Source note | uspto-grants-2009_04 |