HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzenesulfonyl Chloride → HCID 9846776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzenesulfonyl Chloride | HCID 2734258 | — |
| Reactant | 2'-Aminomethylbiphenyl-2-carboxylic acid (3-methylbutyl)amide | HCID 67316109 | — |
| Reactant | HCID 86589514 | HCID 86589514 | — |
| Product | HCID 9846776 | HCID 9846776 | — |
Reaction Steps
From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid (3-methyl-butyl)amide (precursor 5c) and 3-fluorophenylsulfonyl chloride, according to the general working procedure 118 mg of 2′-(3-fluorophenylsulfonyl-aminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained; m.p. 141° C. MS (ES+): m/e=455 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514582B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-f9b10071d3f64b53b8c0d7e3a23eb334 |
| Source note | uspto-grants-2009_04 |