HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Propanesulfonyl chloride → HCID 9887383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Propanesulfonyl chloride | HCID 82408 | — |
| Reactant | 2'-Aminomethylbiphenyl-2-carboxylic acid (3-methylbutyl)amide | HCID 67316109 | — |
| Product | HCID 9887383 | HCID 9887383 | — |
Reaction Steps
From 0.34 mmol of 2′-aminomethylbiphenyl-2-carboxylic acid (3-methyl-butyl)amide (precursor 5c) and isopropylsulfonyl chloride, according to the general working procedure followed by purification by flash chromatography 16 mg of 2′-(isopropylsulfonylaminomethyl)biphenyl-2-carboxylic acid (3-methylbutyl)amide were obtained as an oil. MS (ES+): m/e 403 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514582B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-24b280622ef947ad85e2bf871e8cf43a |
| Source note | uspto-grants-2009_04 |