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HRID2109556

反应详情

EQUATION

反应方程式

HRID 2109556 的结构方程式

REACTANTS

反应物

2
反应SMILES：NCCc1ccccn1
HCID75919

2-(2-Aminoethyl)pyridine

C7H10N2

反应SMILES：O=C(NCc1ccccc1-c1ccccc1C(=O)O)OCc1ccccc1
HCID10915393

未命名化合物

PRODUCTS

产物

1
反应SMILES：O=C(NCc1ccccc1-c1ccccc1C(=O)NCCc1ccccn1)OCc1ccccc1
HCID656730

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCCCCCC.CCOC(C)=O
溶剂HCID21899848

未命名化合物

PROCEDURE

实验过程

From 0.28 mmol of 2′-(benzyloxycarbonylaminomethyl)biphenyl-2-carboxylic acid (precursor 6) and 2-(2-pyridyl)ethylamine, according to ,the general working procedure and subsequent purification by flash chromatography 85 mg of 2′-(benzyloxycarbonylaminomethyl)biphenyl-2-carboxylic acid 2-(2-pyridyl)ethylamide were obtained; m.p. 140° C. (heptane/EA); MS (ES+): m/e=466 (M+1).

WORKUP

后处理

  1. customgeneral working procedure and subsequent purification by flash chromatography 85 mg of 2′-(benzyloxycarbonylaminomethyl)biphenyl-2-carboxylic acid 2-(2-pyridyl)ethylamide
  2. customwere obtained