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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2109556Generated: October 30, 2026

2-Pyridineethanamine → S9947

https://huagongshe.com/reaction/2109556

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-PyridineethanamineHCID 75919—
Reactant2'-(Benzyloxycarbonylaminomethyl)biphenyl-2-carboxylic acidHCID 10915393—
SolventEthylacetate heptaneHCID 21899848—
ProductS9947HCID 656730—

Reaction Steps

From 0.28 mmol of 2′-(benzyloxycarbonylaminomethyl)biphenyl-2-carboxylic acid (precursor 6) and 2-(2-pyridyl)ethylamine, according to ,the general working procedure and subsequent purification by flash chromatography 85 mg of 2′-(benzyloxycarbonylaminomethyl)biphenyl-2-carboxylic acid 2-(2-pyridyl)ethylamide were obtained; m.p. 140° C. (heptane/EA); MS (ES+): m/e=466 (M+1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07514582B2
Source datasetuspto-grants-2009_04
ORD IDord-9790f934e0a54cfdae806ea339ceee0b
Source noteuspto-grants-2009_04