HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21959667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 10160462 | HCID 10160462 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21959667 | HCID 21959667 | — |
Reaction Steps
N-(1-Acetyl-3,3-dimethyl-2,3-dihydro-1H-indol-6-yl)-2-(1H-indazol-6-ylamino)-nicotinamide (500 mg) was deprotected heating with 12 N HCl (3 ml) and EtOH (3 ML) at reflux for 1 h. Dried under vacuum and purified via HPLC. M+H 399.3; Calc'd for C23H22N6O: 398.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07514564B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-1f3b006d0983491fb4c61ab77d696004 |
| Source note | uspto-grants-2009_04 |