HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperazine → HCID 135481186, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperazine | HCID 4837 | — |
| Reactant | HCID 827174 | HCID 827174 | — |
| Product | HCID 135481186 | HCID 135481186 | 55.4% |
Reaction Steps
8-Chloro-2-methoxy-5,10-dihydro-dibenzo[b,e][1,4]diazepine-11-one (28 mg, 0.1 mmol) and piperazine (86 mg, 1.0 mmol) were reacted according to GP4 to give 19 mg of the title compound (160FE20A). MS (ESI) 342 (MH+). Purity for MH+ (UV/MS) 99/100.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517871B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-3d3887285d6f477a9072d72422b5996a |
| Source note | uspto-grants-2009_04 |