HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dimethylethyl 2-(4-piperidinyl)hydrazinecarboxylate → HCID 136029241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dimethylethyl 2-(4-piperidinyl)hydrazinecarboxylate | HCID 67159281 | — |
| Reactant | HCID 136056013 | HCID 136056013 | — |
| Product | HCID 136029241 | HCID 136029241 | 18.1% |
Reaction Steps
8-Chloro-11-methylsulfanyl-5H-dibenzo[b,e][1,4]diazepine (166JO50) (50 mg, 0.11 mmol) and 4-(tert-butoxycarbonylamino)aminopiperidine (39 mg, 0.2 mmol) were reacted according to GP8 to give 6.5 mg of the title compound (166JO55). MS (ESI) 327 (MH+). Purity for MH+ (UV/MS) 100/99.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517871B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-69b00fb721794bd3ab128ba8d1840244 |
| Source note | uspto-grants-2009_04 |