HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68631976, compound → HCID 178477857, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68631976 | HCID 68631976 | — |
| Reactant | HCID 136056013 | HCID 136056013 | — |
| Product | HCID 178477857 | HCID 178477857 | 11.2% |
Reaction Steps
8-Chloro-11-methylsulfanyl-5H-dibenzo[b,e][1,4]diazepine (166JO50) (100 mg, 0.22 mmol) and 3-amino-1-N-(tert-butoxycarbonylamino)pyrrolidine (73 mg, 0.4 mmol) were reacted according to GP8 to give 7.7 mg of the title compound (166JO74). MS (ESI) 313 (MH+). Purity for MH+ (UV/MS) 100/90.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517871B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-4d400198c8cb4dc1a87fb44599eeb851 |
| Source note | uspto-grants-2009_04 |