Dimethyl Sulfate → HCID 86621483, compound

Participants

Reaction Steps

4.88 g (20 mmol) of the compound from Step 3.1 was dissolved with agitation in 60 mL of ethyl acetate and to the solution was added 2.78 g (20 mmol) of dimethyl sulfate. A colorless precipitate formed gradually. The mixture was allowed to agitate for an additional 4 hours at room temperature after which it was filtered, and the filter cake was washed with a small amount of ethyl acetate and then dried at 40° C. under vacuum.

Provenance & Evidence