HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86621483, compound → HCID 86760843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86621483 | HCID 86621483 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86760843 | HCID 86760843 | — |
Reaction Steps
3.7 g (10 mmol) of the compound from Step 3.2 was hydrogenated in 25 mL of water in the presence of 0.3 g of Pd/C (10%) under 9 bar of hydrogen pressure. After 2 hours, the catalyst was filtered off, and the solution obtained was directly subjected to further reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517367B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-6958194011a746a2ab011163945d77af |
| Source note | uspto-grants-2009_04 |