HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86069942, compound → HCID 86069945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86069942 | HCID 86069942 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86069945 | HCID 86069945 | — |
Reaction Steps
4.0 g (12 mmol) of the compound from Step 12.2 in 80 mL of water was hydrogenated in the presence of 0.4 g of Pd/C (10%) under 9 bar of hydrogen pressure. After 3 hours the catalyst was filtered off and the water was removed in a rotary evaporator.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517367B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-6afdf3c9030f4b3aaac4b41695338fed |
| Source note | uspto-grants-2009_04 |