HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(3-Fluorophenyl)-6-nitropyridin-3-amine → HCID 28477225, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(3-Fluorophenyl)-6-nitropyridin-3-amine | HCID 57636791 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 28477225 | HCID 28477225 | 98.4% |
Reaction Steps
This compound was easily prepared from N-(3-fluorophenyl)-6-nitro-3-pyridinamine 210 mg, 0.9 mmol) by catalytic hydrogenation (Raney nickel at atmospheric pressure) in methanol to give the desired product (180 mg, 98%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07517992B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-394ad5acd5af44be9d8edd28a851fb3f |
| Source note | uspto-grants-2009_04 |