HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86603558, compound → HCID 68919313, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86603558 | HCID 86603558 | — |
| Solvent | Propylamine | HCID 7852 | — |
| Product | HCID 68919313 | HCID 68919313 | 169.6% |
Reaction Steps
5,6-Dimethyl-2-(3-pyridyl)-3-mesyloxyethylisoindolin-1-one (0.11 g, 0.31 mmol) was stirred in n-propylamine (3 ml) at 25° C. for 6 hrs. The reaction solution was concentrated under reduced pressure, and the residue was purified by silica gel chromatography (chloroform:methanol=15:1) to give 85 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07521451B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-813d2aca12dd4d15904ece5d11bfa43d |
| Source note | uspto-grants-2009_04 |